Closely follows an actual structural determination. After some introductory material on the nature of x–rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x–ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x–ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
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Titolo: X–Ray Structure Determination
Autore:
Jensen Lyle H.,
Stout George H.
Editore: Wiley–Blackwell
Data di Pubblicazione: 1989
Pagine: 480
Formato: Copertina rigida
ISBN: 9780471607113